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Thorough study of the TEM photos (G) out of graphite needles within the examples growing just after 8 min in the 2nd growing process at the step one,600 W clearly showcases the brand new stage transformation procedure away from graphite to help you diamond. The newest light boxes would be the section to your related increased photographs and you can FFT images less than, plus the purple and you may light arrows imply the brand new plane point. (H) and (H-1) are the HADDF and you will brilliant career TEM pictures for the next graphite needle, correspondingly, to the associated enlarged photographs and you can FFT photographs below. The brand new EELS spectra (I) of the additional internet sites marked because of the red-colored things away from other stage changing needle found in the (H)/(H-1).

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(J)/(J-1) Design of the phase sales away from graphite to help you diamond from the graphite needle adult for the cauliflower-for example dust. To know so it incredible periodicity developing process, HRTEM proportions for the recently shaped coating were performed (Fig. 2). The fresh 0-s sample (Fig. 2A) displays higher pole-including diamond crystals evidenced by the diffraction locations on the diamond (111) orientation in the inset Fourier change (FFT) picture.

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